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Norm

ISO 3196:1975

Issue date: 1975 05 01

Sodium hydroxide for industrial use — Determination of carbonates content — Titrimetric method

Applicable to products having contents, expressed as CO2 , of more than 0.01 % (m/m). Relates to a procduct containing neither sulphides nor chlorates or only sulphides o...
Valid
Publisher:
International Organization for Standardization
Format:
Digital | 4 Pages
Language:
English

Applicable to products having contents, expressed as CO2 , of more than 0.01 % (m/m). Relates to a procduct containing neither sulphides nor chlorates or only sulphides or only chlorates. Preliminary test by boiling an acidified test sample in the presence of methyl orange and with a lead acetate paper strip in the vapour. The sulphides blacken the paper and chlorates delolourize the methyl orange. Products containing neither sulphides nor chlorates: liberation of carbon dioxide by acidification and heating. Entrainment in a flow of gas and absorption in an excess of barium hydroxide solution. Titration of the excess barium hydroxide solution with a standard volumetric hydrochloric acid solution in the presence of thymolphthalein as indicator.